===================== Product Identification =====================
MSDS NAME:SO-K-3 (KARL FISCHER REAGENT)
NIIN:00-084-9334
MSDS Number: BCYDX
=== Responsible Party ===
Company:FISHER SCIENTIFIC COMPANY
Address:1 REAGENT LANE
City:FAIR LAWN
State:NJ
ZIP:07410
Country:US
Info Phone Num:201-796-7100
Emergency Phone Num:201-796-7100 OR 201-796-7523
CAGE:1B464
=== Contractor Identification ===
Company:FISHER SCIENTIFIC CO. CHEMICAL MFG DIV
Address:1 REAGENT LANE
Box:City:FAIRLAWN
State:NJ
ZIP:07410-2802
Country:US
Phone:201-796-7100
CAGE:1B464
============= Composition/Information on Ingredients =============
Name:2-METHOXYETHANOL (EGME) (SARA III)
CAS:109-86-4
RTECS #:KL5775000
= Wt:43.
OSHA PEL:S, 25 PPM
ACGIH TLV:S, 5 PPM; 9192
Name:PYRIDINE (SARA III)
CAS:110-86-1
RTECS #:UR8400000
= Wt:43.
OSHA PEL:5 PPM
ACGIH TLV:5 PPM; 9192
EPA Rpt Qty:1000 LBS
DOT Rpt Qty:1000 LBS
Name:IODINE
CAS:7553-56-2
RTECS #:NN1575000
= Wt:13.8
OSHA PEL:C 0.1 PPM
ACGIH TLV:C 0.1 PPM; 9192
Name:SULFUR DIOXIDE (SARA III)
CAS:7446-09-5
RTECS #:WS4550000
= Wt:.1
OSHA PEL:5 PPM/5 STEL
ACGIH TLV:2 PPM/5 STEL; 9293
===================== Hazards Identification =====================
Effects of Overexposure:IRRITATS SKIN;CAN CAUSE CNS DEPRES;HARMFUL IF
SWALLOWED,INHALED OR ABSORBED THROUGH SKIN.
======================= First Aid Measures =======================
First Aid:DANGER! MAY BE FATAL IF SWALLOWED.AVOID PROLONGED BREATHING
OF VAPOR.USE WITH ADEQUATE VENTILATION. ANTIDOTE:EXTERNAL - WASH
WITH PLENTY OF WATER; INTERNAL-GIVE SODIUM THIOSULFATE.1 TBSP IN A
GLASS OF WATER. OR STARCH PASTE. SEE SUPP DATA
===================== Fire Fighting Measures =====================
Flash Point Method:CC
Flash Point:=50.6C, 123.F
Lower Limits:UNK
Upper Limits:UNK
Extinguishing Media:CO*2, DRY CHEMICAL, WATER SPRAY
Fire Fighting Procedures:USE H*20 TO COOL EXPD CONTRS. USE SCBA & FULL
PROT.CLTHG.
Unusual Fire/Explosion Hazard:TOXIC VAPORS ARE LIBERATED DURING
COMBUSTION.
================== Accidental Release Measures ==================
Spill Release Procedures:LIQ SPILL: STOP LEAK,ELIMINATE IGNITION
SOURCES. COVER W SODIUM BICARBONATE/SLAKED LIME MIX (50-50).MIX
AND ADD WATER IF NECESSARY TO MAKE SLURRY. WASH THROUGH DRAIN W
EXCESS H*2O.
====================== Handling and Storage ======================
Handling and Storage Precautions:STORE IN A COOL, DRY PLACE, TIGHTLY
CAPPED AND AWAY FROM FLAMES,SPARKS AND FIRE HAZARDS
Other Precautions:NOT KNOWN
============= Exposure Controls/Personal Protection =============
Respiratory Protection:WEAR SELF-CNTND BRTHG APP
Ventilation:MECHANICAL(GENERAL) RECOMMENDED,LOCAL EXHAUST IF NEEDED
Protective Gloves:RUBBER
Eye Protection:SAFETY GOGGLES
Other Protective Equipment:RUBBER APRON
Supplemental Safety and Health
FIRST AID CONT:FOLLOW W WARM SALT WATER UNTIL VOMIT FLUID IS CLEAR.THEN
GIVE MILK OR EGG WHITES BEATEN W WATER.CALL DR.;PRODUCT IS SINGLE
SOLUTION STABILIZED KARL FISHER REAGENT.
================== Physical/Chemical Properties ==================
HCC:F5
NRC/State Lic Num:NOT RELEVANT
Boiling Pt:B.P. Text:115-125C
Vapor Pres:UNK
Vapor Density:UNK
Spec Gravity:1.16
Evaporation Rate & Reference:>1(ETHER=1)
Solubility in Water:COMPLETE
Appearance and Odor:DARK BROWN LIQUID;IRRITATING PUNGENT PYRIDINE ODOR
Percent Volatiles by Volume:70
================= Stability and Reactivity Data =================
Stability Indicator/Materials to Avoid:YES
NONE
Stability Condition to Avoid:HIGH TEMPERATURES,IGNITION SOURCES
Hazardous Decomposition Products:EMITS TOXIC VAPS OF IODINE & SULFUR
OXIDES WHEN HEATED.
==================== Disposal Considerations ====================
Waste Disposal Methods:WEAR RUBBER CLOVES,SCBA, PROTECT CLTHG. ADD
SLOWLY TO LG VOL OF AGITATED SOLN OF NA*2 CO*2 & CA(OH)*2. ADD THIS
SOLN TO LG EXCESS OF H*20. ELIM IGN SOURCES OR KEEP IN COVD DRS.
HDLE & DISPOSE LW ALL APPL INTERN, FED, STATE & LOCAL REGS.
Disclaimer (provided with this information by the compiling agencies):
This information is formulated for use by elements of the Department
of Defense. The United States of America in no manner whatsoever,
expressly or implied, warrants this information to be accurate and
disclaims all liability for its use. Any person utilizing this
document should seek competent professional advice to verify and
assume responsibility for the suitability of this information to their
particular situation.
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