EPA Method 1618
Method 1618
Organo-halide & Organo-phosphorus Pesticides & Phenoxyacid Herbicides
Method 1618 was developed by the Industrial Technology Division (ITD) within the United States Environmental Protection
Agency’s (US EPA) Office of Water Regulations and Standards (OWRS) to provide improved precision and accuracy of analysis of
pollutants in aqueous and solid matrices in order to determine the level of these pollutants in industrial discharges.
Method 1618 is used with wide bore GC columns to analyze for organo-halide and organo-phosphorus pesticides, phenoxy-acid
herbicides and herbicide esters, polychlorinated biphenyls (PCBs) and other compounds amenable to extraction and analysis by
wide bore capillary column gas chromatography with halogen-specific and organo-phosphorus detectors.
The chemical compounds in the AccuStandard mixtures that follow may be determined in waters, soils, sediments and sludges by
this method. The method is a consolidation of EPA Methods 608, 608.1, 614, 615, 617, 622 and 701.
Method 1618 Organo-halide Pesticides, Organo-phosphorus Pesticides and Phenoxyacid Herbicides by
Wide Bore Capillary Column Gas Chromatography
Organochlorine Pesticides Phenoxyacid Herbicides
M-1618-1 $ 75 / 1 x 1 mL M-8150M $ 40 / 1 x 1 mL
M-1618-1-PAK SAVE 20% $ 300 / 5 x 1 mL M-8150M-PAK SAVE 20% $ 160 / 5 x 1 mL
At stated conc. in Isooctane 14 comps. 20 µg/mL each in Hexane 8 comps.
2,4-D 2,4,5-TP Dichlorprop
Aldrin (100 ng/mL) Endosulfan II (200 ng/mL)
2,4-DB Dalapon Dinoseb
Captan (200 ng/mL) Endrin aldehyde (100 ng/mL)
2,4,5-T Dicamba
Chlorobenzilate (500 ng/mL) Heptachlor (100 ng/mL)
Diallate (250 ng/mL) Heptachlor epoxide (100 ng/mL)
p,p�-DDE (200 ng/mL) Lindane (100 ng/mL) M-8150M-2 $ 15 / 1 x 1 mL
p,p�-DDT (200 ng/mL) Methoxychlor (200 ng/mL) M-8150M-2-PAK SAVE 20% $ 60 / 5 x 1 mL
Endosulfan I (200 ng/mL) Isodrin (100 ng/mL) 2.0 mg/mL in Hexane 2 comps.
MCPA MCPP
Organochlorine Pesticides
Surrogate Standards
M-1618-2 $ 75 / 1 x 1 mL
At stated conc. in Isooctane 16 comps.
Organochlorine Pesticide
M-1618-SS $ 15 / 1 x 1 mL
(100 ng/mL) Dichlone (100 ng/mL)
α-BHC
M-1618-SS-PAK SAVE 20% $ 60 / 5 x 1 mL
(100 ng/mL) Dieldrin (100 ng/mL)
β-BHC
2 µg/mL in Acetone
(100 ng/mL) Endrin (100 ng/mL)
δ-BHC
(100 ng/mL) Endosulfan sulfate (100 ng/mL)
αChlordane
Dibutylchlorendate
(100 ng/mL) Endrin ketone (100 ng/mL)
γ-Chlordane
Carbophenothion (1000 ng/mL) Mirex (100 ng/mL)
Captafol (200 ng/mL) PCNB (100 ng/mL) Organophosphate Pesticide
p,p�-DDD (100 ng/mL) Trifluralin (200 ng/mL)
M-1618-SP $ 20 / 1 x 1 mL
2 µg/mL each in Acetone 2 comps.
Organophosphate Pesticides Tributyl phosphate Triphenyl phosphate
M-1618-3 $ 90 / 1 x 1 mL
At stated conc. in Isooctane 19 comps.
Phenoxyacid Herbicide
Azinphos methyl (100 ng/mL) Merphos (200 ng/mL) M-1618-SA $ 10 / 1 x 1 mL
Coumaphos (50 ng/mL) Methyl parathion (100 ng/mL) 2 µg/mL in Acetone
Diazinon (100 ng/mL) Malathion (100 ng/mL)
Dacthal (2,4-Dichlorophenyl acetic acid)
Dichlorvos (50 ng/mL) Phorate (100 ng/mL)
Dimethoate (100 ng/mL) Ronnel (100 ng/mL)
EPN (100 ng/mL) Sulprofos (50 ng/mL)
Ethyl parathion (100 ng/mL) Terbufos (100 ng/mL) Decomposition Solution
Ethoprop (100 ng/mL) Tetrachlorvinphos (100 ng/mL) M-1618D $ 15 / 1 x 1 mL
Ethyl azinphos (100 ng/mL) Trichlorofon (100 ng/mL) M-1618D-PAK SAVE 20% $ 60 / 5 x 1 mL
Fensulfothion (200 ng/mL) At stated conc. in Acetone 2 comps.
p,p�-DDT (2.0 µg/mL) Endrin (1.0 µg/mL)
Organophosphate Pesticides
M-1618-4 $ 90 / 1 x 1 mL
GPC Calibration Solution
At stated conc. in Isooctane 16 comps.
M-1618-GP-5ML $ 35 / 1 x 5 mL
At stated conc. in Acetone 5 comps.
Chlorfenvinphos (50 ng/mL) Ethion (100 ng/mL)
Chlorpyrifos (50 ng/mL) Famphur (200 ng/mL) Corn oil (300.0 mg/mL) Perylene (0.1 mg/mL)
Chlorpyrifos methyl (100 ng/mL) Fenthion (100 ng/mL) bis(2-Ethylhexyl)phthalate (15.0 mg/mL) Sulfur (0.5 mg/mL)
Crotoxyphos (200 ng/mL) Leptophos (100 ng/mL) Pentachlorophenol (1.4 mg/mL)
Dichlorofenthion (100 ng/mL) Mevinphos (100 ng/mL)
Demeton (400 ng/mL) Naled (100 ng/mL)
SPE Cartridge Calibration Solution
Dioxathion (600 ng/mL) Phosmet (200 ng/mL)
Disulfoton (100 ng/mL) Sulfotep (50 ng/mL) M-1618-SE $ 10 / 1 x 1 mL
M-1618-SE-PAK SAVE 20% $ 40 / 5 x 1 mL
0.1 µg/mL in Acetone
2,4,6-Trichlorophenol
214 Quality System is Certified to comply with the International ISO 9001 Quality Standard
EPA Method 1653 Method 1653
Method 1653 is designed to determine Chlorinated Phenolics (chlorinated phenols, guaiacols, catechols, vanillins,
syringaldehydes) and other compounds in wastewater amenable to in-situ acetylation and analysis by GC/MS.
Method 1653 Chlorinated Phenolics in Pulp and Paper Effluents
M-1653A-D-R-SET $ 250 / set of 4 x 1 mL M-1653A-D-R2-SET $ 250 / set of 4 x 1 mL
Method 1618-1653
(set includes M-1653A, B, C, D-AC) (set includes M-1653A-R, B-R, C-R, D-R)
M-1653A $ 25 / 1 x 1 mL M-1653A-R $ 25 / 1 x 1 mL
M-1653A-PAK SAVE 20% $ 100 / 5 x 1 mL At stated conc. in Acetone 7 comps.
0.1 mg/mL each in MeOH 7 comps.
4-Chlorophenol 2,4,6-Trichlorophenol 4-Chlorophenol (25 µg/mL) 2,4,6-Trichlorophenol (50 µg/mL)
2,4-Dichlorophenol 2,3,4,6-Tetrachlorophenol 2,4-Dichlorophenol (50 µg/mL) 2,3,4,6-Tetrachlorophenol (50 µg/mL)
2,6-Dichlorophenol Pentachlorophenol 2,6-Dichlorophenol (50 µg/mL) Pentachlorophenol (100 µg/mL)
2,4,5-Trichlorophenol 2,4,5-Trichlorophenol (50 µg/mL)
M-1653B-R $ 125 / 1 x 1 mL
M-1653B $ 125 / 1 x 1 mL
At stated conc. in Acetone 8 comps.
0.1 mg/mL each in MeOH 8 comps.
3,4,5-Trichloroguaiacol (50 µg/mL)
4-Chloroguaiacol (25 µg/mL)
4-Chloroguaiacol 3,4,5-Trichloroguaiacol
3,4,6-Trichloroguaiacol (50 µg/mL)
3,4-Dichloroguaiacol (50 µg/mL)
3,4-Dichloroguaiacol 3,4,6-Trichloroguaiacol
4,5,6-Trichloroguaiacol (50 µg/mL)
4,5-Dichloroguaiacol (50 µg/mL)
4,5-Dichloroguaiacol 4,5,6-Trichloroguaiacol
Tetrachloroguaiacol (100 µg/mL)
4,6-Dichloroguaiacol (50 µg/mL)
4,6-Dichloroguaiacol Tetrachloroguaiacol
M-1653C $ 95 / 1 x 1 mL M-1653C-R $ 95 / 1 x 1 mL
0.1 mg/mL each in MeOH 7 comps. At stated conc. in Acetone 7 comps.
4-Chlorocatechol 3,4,5-Trichlorocatechol 4-Chlorocatechol (25 µg/mL) 3,4,5-Trichlorocatechol (100 µg/mL)
3,4-Dichlorocatechol 3,4,6-Trichlorocatechol 3,4-Dichlorocatechol (50 µg/mL) 3,4,6-Trichlorocatechol (100 µg/mL)
3,6-Dichlorocatechol Tetrachlorocatechol 3,6-Dichlorocatechol (50 µg/mL) Tetrachlorocatechol (100 µg/mL)
4,5-Dichlorocatechol 4,5-Dichlorocatechol (50 µg/mL)
M-1653D-AC $ 65 / 1 x 1 mL M-1653D-R $ 65 / 1 x 1 mL
0.1 mg/mL each in Acetone 6 comps. At stated conc. in Acetone 6 comps.
5-Chlorovanillin 2-Chlorosyringaldehyde 5-Chlorovanillin (50 µg/mL) 2-Chlorosyringaldehyde (50 µg/mL)
6-Chlorovanillin 2,6-Dichlorosyringaldehyde 6-Chlorovanillin (50 µg/mL) 2,6-Dichlorosyringaldehyde (100 µg/mL)
5,6-Dichlorovanillin Trichlorosyringol 5,6-Dichlorovanillin (100 µg/mL) Trichlorosyringol (50 µg/mL)
Internal Standard Instrument Internal Standard Instrument Performance
M-1653-IS $ 35 / 1 x 1 mL M-1653-IIS $ 20 / 1 x 1 mL Check Solution
1.0 mg/mL in MeOH 1.0 mg/mL in MeOH
M-1653-TS $ 20 / 1 x 1 mL
50 µg/mL in Acetone
M-1653-IS-R $ 35 / 1 x 1 mL M-1653-IIS-R $ 25 / 1 x 1 mL
1.0 mg/mL in Acetone 5.0 mg/mL in Acetone
DFTPP
3,4,5-Trichlorophenol 2,2'-Difluorobiphenyl
AccuSnapâ„?
For your Safety, helps protect your hands!
AccuSnap, included at no charge with AccuPAKs (5 x 1 mL), is
designed to protect against cuts while breaking open ampules.
Easy to use! Simply place over the ampule, slide below the score
line, and snap the ampule neck. The AccuSnap is made of a heavy
gauge, durable and flexible plastic.
215
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EPA Method 1656
Method 1656
CC
C Ready-to-Inject Working Level Pesticide Standards
Method 1656 is a consolidation of several EPA wastewater Working Level Continuing Calibration Check Standards
methods used to determine the organo-halide pesticides and (CCC) for the 1600 MethodSeries
polychlorinated biphenyls (PCBs) associated with the Clean AccuStandard has expanded the existing pesticide standard product
Water Act, the Resource Conservation and Recovery Act, and line to include the new working level Continuing Calibration Check
the Comprehensive Environmental Response, Compensation Standard Line (CCC Line) for EPA 1600 series methods. The new
and Liability Act; and other compounds amenable to extraction working level (CCC Line) revolutionizes the way the analytical chemist
prepares standards for pesticide analysis:
and analysis by wide-bore capillary column gas
chromatography with a halogen specific detector (HSD). All necessary standards are provided to begin instrument
calibration.
No dilutions are required to make the 3 point curve.
Method 1656 Organo-Halide Pesticides in
Allows direct transfer of the standard to the auto sampler vials.
Municipal & Industrial Wastewater
The internal standard or surrogate is already incorporated in
the standard.
GPC Calibration Solution
M-1600-GPC-5ML $ 35 / 1 x 5 mL Convenient packaging reduces disposal costs.
At stated conc. in CH2Cl2 5 comps.
Cost effective. Time is spent quantifying samples, which
Corn oil (300 mg/mL) Perylene (0.1 mg/mL) generate revenue rather than preparing standards.
bis(2-Ethylhexyl)phthalate (15 mg/mL) Sulfur (0.5 mg/mL)
Pentachlorophenol (1.4 mg/mL)
Method 1656 Calibration Solutions and Suggested
Calibration Groups
Solid-phase Extraction Cartridge Calibration
Solution M-1656-CAL-SET $ 360 / 7 x ( 3 x 1 mL )
(contains all 7 calibration groups at
M-1600-SPE $ 10 / 1 x 1 mL
respective low, medium and high ranges)
0.1 mg/mL in Acetone
2,4,6-Trichlorophenol
Calibration Group 1
M-1656-01-CAL-SET $ 75 / 3 x 1 mL
Surrogate Spiking Solutions All solutions in Isooctane 14 comps.
CLP-PES-A $ 15 / 1 x 1 mL
M-1 M-1 M- 1
0.2 mg/mL in Acetone 6 56 6 56 656
-01- -01- -01-
1X 5X 20X
Cat. No.
Dibutylchlorendate
Components Low Medium High
CLP-032R $ 15 / 1 x 1 mL (units in ng/mL) ( 1X ) ( 5X ) ( 20X )
0.2 mg/mL each in Acetone 2 comps.
Acephate 2,000 10,000 40,000
Decachlorobiphenyl Tetrachloro-m-xylene Alachlor 20 100 400
Atrazine 1,000 5,000 20,000
10 50 200
β-BHC
CLP-034 $ 15 / 1 x 1 mL Bromoxynil octanoate 50 250 1,000
0.2 mg/mL each in Acetone 2 comps. Captafol 200 1,000 4,000
Diallate 200 1,000 4,000
Dibutylchlorendate Tetrachloro-m-xylene Decachlorobiphenyl 10 50 200
Endosulfan sulfate 10 50 200
Endrin 20 100 400
Decomposition Test Solution Isodrin 10 50 200
M-1656-DS $ 15 / 1 x 1 mL Pendimethalin 50 250 1,000
At stated conc. in Isooctane 2 comps. Permethrin (cis & trans) * 200 1,000 4,000
Tetrachloro-m-xylene 5 25 100
4,4'-DDT (2 µg/mL) Endrin (1 µg/mL)
* Actual isomer concentration is stated on certificate of product data
Calibration Solutions & Suggested Calibration Groups
Continued on Next page
Ready-to-Inject
Working Level Standards &
Continuing Calibration Check (CCC)
216 Quality System is Certified to comply with the International ISO 9001 Quality Standard
EPA Method 1656 Method 1656
(cont'd)
CC
C
Ready-to-Inject Working Level Pesticide Standards
Method 1656 Calibration Solutions and Suggested Calibration Groups (Continued)
Calibration Group 2 Calibration Group 5
M-1656-02-CAL-SET $ 60 / 3 x 1 mL M-1656-05-CAL-SET $ 60 / 3 x 1 mL
All solutions in Isooctane 11 comps. All solutions in Isooctane 8 comps.
M-1 M-1 M- 1 M-1 M-1 M- 1
656 65 6 6 56 65 6 6 56 6 56
-02- -02- -02-
Method 1656
-05- -05- -05-
1X 5X 2 0X 1X 5X 20X
Cat. No.
Cat. No.
Components Low Medium High Components Low Medium High
(units in ng/mL) ( 1X ) ( 5X ) ( 20X ) (units in ng/mL) ( 1X ) ( 5X ) ( 20X )
5 25 100
α-BHC Benfluralin 20 100 400
DCPA 5 25 100 Captan 100 500 2,000
4,4'-DDE 10 50 200 Chlorothalonil 20 100 400
4,4'-DDT 10 50 200 4,4'-DDD 20 100 400
Decachlorobiphenyl 10 50 200 Decachlorobiphenyl 10 50 200
Dichlone 20 100 400 Norflurazon 100 500 2,000
Ethalfluralin 10 50 200 Simazine 800 4,000 16,000
Fenarimol 20 100 400 100
Tetrachloro-m-xylene 5 25
Methoxychlor 20 100 400
Metribuzin 10 50 200
Tetrachloro-m-xylene 5 25 100
Calibration Group 6
M-1656-06-CAL-SET $ 60 / 3 x 1 mL
Calibration Group 3 All solutions in Isooctane 9 comps.
M-1656-03-CAL-SET $ 60 / 3 x 1 mL
M-1 M-1 M- 1
All solutions in Isooctane 10 comps.
65 6 656 6 56
-06- -06- -06-
1X 5X 2 0X
M-1 M-1 M- 1 Cat. No.
6 56 65 6 656
-03- -03- -03-
1X 5X 20 X
Cat. No. Components Low Medium High
(units in ng/mL) ( 1X ) ( 5X ) ( 20X )
Components Low Medium High
Aldrin 20 100 400
(units in ng/mL) ( 1X ) ( 5X ) ( 20X )
5 25 100
δ-BHC
Bromacil 100 500 2,000
5 25 100
γ-BHC
Butachlor 50 250 1,000
5 25 100
γ-Chlordane
Decachlorobiphenyl 10 50 200
Decachlorobiphenyl 10 50 200
Endosulfan II 10 50 200
Endrin ketone 10 50 200
Heptachlor 10 50 200
Heptachlor epoxide 5 25 100
Kepone 100 500 2,000
Isopropalin 20 100 400
Tetrachloro-m-xylene 5 25 100
Nitrofen 20 100 400
PCNB 5 25 100
Tetrachloro-m-xylene 5 25 100
Trifluralin 10 50 200
Calibration Group 7
M-1656-07-CAL-SET $ 75 / 3 x 1 mL
All solutions in Isooctane 13 comps.
Calibration Group 4 M-1 M-1 M- 1
656 6 56 656
-07- -07- -07-
M-1656-04-CAL-SET $ 60 / 3 x 1 mL 1X 5X 20X
Cat. No.
All solutions in Isooctane 10 comps.
M-1 M-1 M- 1
6 56 65 6 656 Components Low Medium High
-04- -04- -04-
1X 5X 20X (units in ng/mL) ( 1X ) ( 5X ) ( 20X )
Cat. No.
Carbophenothion 80 400 1,600
Components Low Medium High Chloroneb 300 1,500 6,000
(units in ng/mL) ( 1X ) ( 5X ) ( 20X ) Chloropropylate 200 1,000 4,000
DBCP 25 125 500
Benfluralin 20 100 400 Decachlorobiphenyl 10 50 200
Chlorobenzilate 50 250 1,000 Dicofol 300 1,500 6,000
Decachlorobiphenyl 10 50 200 Endrin aldehyde 80 400 1,600
Dieldrin 5 25 100 Etridiazole 80 400 1,600
Endosulfan I 10 50 200 Perthane 1,000 5,000 20,000
Mirex 20 100 400 Propachlor 500 2,500 10,000
Terbacil 200 1,000 4,000 Propanil 200 1,000 4,000
Terbuthylazine 500 2,500 10,000 Propazine 1,000 5,000 20,000
Tetrachloro-m-xylene 5 25 100 Tetrachloro-m-xylene 5 25 100
Triadimefon 100 500 2,000
217
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EPA Method 1657
Method 1657
CC
C Ready-to-Inject Working Level Pesticide Standards
Method 1657 is a consolidation of several EPA wastewater methods used to determine the organo-phosphorus pesticides
associated with the Clean Water Act, the Resource and Conservation and Recovery Act, and the Comprehensive Environmental
Response, Compensation and Liability Act; and other compounds amenable to extraction and analysis by wide-bore capillary column
gas chromatography with a flame photometric detector (FPD).
Method 1657 The Determination of Organo-Phosphorus Pesticides in Municipal & Industrial Wastewaste
GPC Calibration Solution Solid-phase Extraction Cartridge Surrogate Spiking Solution
M-1600-GPC-5ML $ 35 / 1 x 5 mL M-1657-SS $ 20 / 1 x 1 mL
Calibration Solution
At stated conc. in CH2Cl2 5 comps. 0.2 mg/mL each in Acetone 2 comps.
M-1600-SPE $ 10 / 1 x 1 mL
Corn oil (300 mg/mL) 0.1 mg/mL in Acetone Tributyl phosphate
bis(2-Ethylhexyl)phthalate (15 mg/mL) Triphenyl phosphate
2,4,6-Trichlorophenol
Pentachlorophenol (1.4 mg/mL)
Perylene (0.1 mg/mL)
Sulfur (0.5 mg/mL)
Method 1657 Calibration Solutions and Suggested Calibration Groups
M-1657-CAL-SET $ 195 / 4 x ( 3 x 1 mL )
Contains all 4 calibration groups at the respective Low, Medium and High Ranges
Calibration Group 3
Calibration Group 1
M-1657-03-CAL-SET $ 60 / 3 x 1 mL
M-1657-01-CAL-SET $ 60 / 3 x 1 mL
All solutions in Isooctane 14 comps.
All solutions in Isooctane 10 comps.
M-1 M-1 M- 1 M-1 M-1 M- 1
657 65 7 657 65 7 657 657
-01- -01- -01- -03- -03- -03-
1X 5X 20X 1X 5X 20X
Cat. No. Cat. No.
Components Low Medium High Components Low Medium High
(units in ng/mL) ( 1X ) ( 5X ) ( 20X ) (units in ng/mL) ( 1X ) ( 5X ) ( 20X )
Azinphos methyl 100 500 2,000 Azinphos ethyl 200 1,000 4,000
Dichlorvos 500 2,500 10,000 Crotoxyphos 500 2,500 10,000
Disulfoton 200 1,000 4,000 DEF 200 1,000 4,000
Fenthion 200 1,000 4,000 Fensulfothion 500 2,500 10,000
Merphos (A + B) 400 2,000 8,000 Methyl chlorpyrifos 200 1,000 4,000
Methyl trithion 500 2,500 10,000 Mevinphos 500 2,500 10,000
Ronnel 200 1,000 4,000 Naled 500 2,500 10,000
Sulprofos 200 1,000 4,000 Parathion 200 1,000 4,000
Tributyl phosphate 200 1,000 4,000 Phosmet 500 2,500 10,000
Triphenyl phosphate 200 1,000 4,000 Phosphamidon (E + Z) 100 500 2,000
Sulfotepp 200 1,000 4,000
Terbufos 200 1,000 4,000
Calibration Group 2 Tributyl phosphate 200 1,000 4,000
Triphenyl phosphate 200 1,000 4,000
M-1657-02-CAL-SET $ 60 / 3 x 1 mL
All solutions in Isooctane 12 comps.
Calibration Group 4
M-1 M-1 M- 1
657 65 7 657
-02- -02- -02- M-1657-04-CAL-SET $ 60 / 3 x 1 mL
1X 5X 20X
All solutions in Isooctane 11 comps.
Cat. No.
M-1 M-1 M- 1
65 7 65 7 657
Components Low Medium High -04- -04- -04-
1X 5X 20X
(units in ng/mL) ( 1X ) ( 5X ) ( 20X )
Cat. No.
Chlorfevinphos 200 1,000 4,000
Components Low Medium High
Chlorpyrifos 200 1,000 4,000
(units in ng/mL) ( 1X ) ( 5X ) ( 20X )
Demeton (O + S) 400 2,000 8,000
Dichlofenthion 200 1,000 4,000
Coumaphos 500 2,500 10,000
Dimethoate 100 500 2,000
Diazinon 200 1,000 4,000
Famphur 500 2,500 10,000
EPN 200 1,000 4,000
Leptophos 200 1,000 4,000
Ethion 200 1,000 4,000
Methyl parathion 200 1,000 4,000
Ethoprop 200 1,000 4,000
Tributyl phosphate 200 1,000 4,000
Malathion 200 1,000 4,000
Trichlorofon 500 2,500 10,000
Phorate 200 1,000 4,000
Tricresylphosphate 100 500 2,000
Tetrachlorvinphos 200 1,000 4,000
Triphenyl phosphate 200 1,000 4,000
Tributyl phosphate 200 1,000 4,000
Trichloronate 200 1,000 4,000
Triphenyl phosphate 200 1,000 4,000
218 Quality System is Certified to comply with the International ISO 9001 Quality Standard
EPA Method 1658/ /1659
EPA Method 1658 1659 Method 1658
1659
CC
C
Ready-to-Inject Working Level Standards
Method 1659 is used to determine Dazomet by base
Method 1658 is part of the consolidation of several EPA
hydrolysis to Methyl Isothiocyanate (MITC) and subsequent
wastewater methods used to determine the Phenoxy-Acid
determination of MITC by wide-bore fused-silica capillary
Herbicides and Herbicide esters associated with the Clean Water
column gas chromatography with a Nitrogen Phophorus
Act, the Resource and Conservation and Recovery Act, and the
Detector (NPD).
Comprehensive Environmental Response, Compensation and
Liability Act; and other compounds amenable to extraction and
Method 1657-1659
analysis by wide-bore capillary column gas chromatography with
a Electron Capture Detector (ECD).
Method 1658 Phenoxy-Acid Herbicides as Method 1659 The Determination of Dazomet
methyl derivatives in Municipal & Industrial Wastewaste
M-1658-CAL-SET $ 75 / 3 x 1 mL Calibration Solutions
All solutions in Isooctane 12 comps.
M-1659-CAL-SET $ 25 / 3 x 1 mL
M-1659-CAL-1X 0.2 mg/mL in Acetone 1 mL
M-1 M- 1 M-1
658 658 658
M-1659-CAL-5X 1.0 mg/mL in Acetone 1 mL
-CA -C A -C A
L-1 L-1 L-1
X 0X 00 M-1659-CAL-25X 5.0 mg/mL in Acetone 1 mL
X
Cat. No.
Methyl isothiocyanate (MITC)
Components
(units in ng/mL) ( 1X ) ( 10X ) ( 100X )
Recovery and Precision Solution
2,4-D 100 1,000 10,000
M-1659-RPS $ 10 / 1 x 1 mL
Dalapon 50 500 5,000
25 µg/mL in Acetone
2,4-DB 200 2,000 20,000
2,4-DCPA (Surrogate) 10 100 1,000
Methyl isothiocyanate (MITC)
Dicamba 20 200 2,000
Dichlorprop 100 1,000 10,000
Dinoseb 50 500 5,000 Matrix Spiking Solution
MCPA 5,000 50,000 500,000
M-1659-MS $ 10 / 1 x 1 mL
MCPP 5,000 50,000 500,000
25 µg/mL in Acetone
Picloram 50 500 5,000
2,4,5-T 20 200 2,000
Dazomet
2,4,5-TP 20 200 2,000
Extensive QC analysis
Technical Note
AccuStandard maintains a full QA/QC
Laboratory with the following types of
instruments to insure the quality of our
standards. GC/FID, GC/ECD, GC/
NPD, GC/MS, P & T GC/MS, HPLC,
and IC.
219
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EPA Method 1665 & 1666A
Method 1665
1666A
Pharmaceutical Waste Discharge Standards
AccuStandard has formulated the following 1600 series Pharmaceutical Manufacturing Industry (PMI) standards to meet methods
promulgated in 40 CFR part 136. These methods are used to monitor the discharge of pollutants into surface waters of the United
States by the Pharmaceutical Manufacturing Industry. The methods can be used to identify and measure purgeable and non-
purgeable volatiles, semi-volatiles, and certain organic pollutants specific to PMI discharge in water, soils, and municipal sludges.
AccuStandard’s PMI standards are formulated at convenient stock and Ready-to-Use concentrations. Further savings can be
achieved by the Analytical Laboratory purchasing the standards in bulk quantities. Contact our Technical Department for a quotation
on those standards available in bulk quantities.
NEW
Method 1665 Semi-Volatile Organic Compounds Specific to the Pharmaceutical Manufacturing Industry (PMI) by
Isotope Dilution GC/MS
PMI Stock Standard
PMI Semi-Volatile Set Instrument Performance Check
M-1665 1 x 1 mL
M-1665-SET $ 320 / 5 x 1 mL Solution
2000 µg/mL each in CH2Cl2 6 comps.
Set includes M-1618-GP-5ML, M-1653-TS
M-1653-TS 1 x 1 mL
M-625-07-10X, M-1665, M-1665-LAB
50 µg/mL in Acetone Aniline Dimethylformamide
N,N-Dimethylacetamide 2-Picoline
DFTPP N,N-Dimethylaniline Pyridine
GPC Calibration Solution
M-1618-GP-5ML 1 x 5 mL
PMI Internal Standard
At stated conc. in Acetone 5 comps.
PMI Labeled Stock Standard
M-625-07-10X 1 x 1 mL
Corn oil (300.0 mg/mL) M-1665-LAB 1 x 1 mL
2.0 mg/mL in CH2Cl2
bis(2-Ethylhexyl)phthalate (15.0 mg/mL) 500 µg/mL each in CH2Cl2 5 comps.
Pentachlorophenol (1.4 mg/mL)
Aniline-d7 2-Picoline-d7
2,2'-Difluorobiphenyl
Perylene (0.1 mg/mL)
N,N-Dimethylaniline-d11 Pyridine-d5
Sulfur (0.5 mg/mL)
Dimethylformamide-d7
Method 1666A Volatile Organic Compounds Specific to the Pharmaceutical Manufacturing Industry (PMI) by NEW
Rev. July 1998 Isotope Dilution GC/MS
PMI Purgeable Analytes PMI Labeled Stock Standard PMI Direct Injection Analytes
M-1666A-SET-R2 $ 240 / 5 x 1 mL M-1666A-LAB 1 x 1 mL
M-1666-DI-R1-SET $ 155 / 4 x 1 mL
Set includes 4 products listed below plus M-1666A-LAB At stated conc. in MeOH 8 comps.
Set includes 4 products listed below
NEW L-Butanol-d10 (500 µg/mL)
M-1666A-SSA-ADD 1 x 1 mL
Cyclohexane-d12 (50 µg/mL)
1000 µg/mL in MeOH
PMI Standard Direct Injection
Ethyl Acetate-c13 (50 µg/mL)
M-1666A-DI-R1 1 x 1 mL
N-Heptane-d16 (50 µg/mL)
Isopropyl ether
At stated conc. in Water 10 comps.
n-Hexane-d14 (50 µg/mL)
Tetrahydrofuran-d8 (50 µg/mL)
Acetonitrile (1000 µg/mL)
PMI Stock Standard A o-Xylene-d10 (50 µg/mL)
Diethylamine (2500 µg/mL)
m-Xylene-d10 (50 µg/mL)
M-1666A-SSA-R2 1 x 1 mL
Dimethylamine (1000 µg/mL)
At stated conc. in MeOH 7 comps.
Dimethyl sulfoxide (1000 µg/mL)
1-Butanol (2500 µg/mL) Ethanol (1000 µg/mL)
PMI Instrument Performance
t-Butanol (2500 µg/mL) Ethylene glycol (2500 µg/mL)
2-Furaldehyde (2500 µg/mL) Methanol (1000 µg/mL)
Isobutyraldehyde (2500 µg/mL) Purgeable Internal Standard 2-Methoxyethanol (1000 µg/mL)
Isopropanol (1000 µg/mL) 1-Propanol (1000 µg/mL)
CLP-PI $ 25 / 1 x 1 mL
4-Methyl-2-pentanone (1000 µg/mL) Triethylamine (2500 µg/mL)
CLP-PI-PAK SAVE 20% $ 100 / 5 x 1 mL
1-Pentanol (2500 µg/mL)
1.0 mg/mL each in MeOH 3 comps.
NEW
Bromochloromethane 1,4-Difluorobenzene
PMI Stock Standard B M-1666A-DI-R1-ADD1 1 x 1 mL
Chlorobenzene-d5
M-1666A-SSB 1 x 1 mL 2500 µg/mL in Water
At stated conc. in MeOH 9 comps.
Cyclohexane (1000 µg/mL) Methylamine
PMI Resolution Standard
N-Heptane (1000 µg/mL)
NEW
M-1666A-RES $ 30 / 1 x 1 mL
n-Hexane (1000 µg/mL)
M-1666A-DI-R1-ADD2 1 x 1 mL
M-1666A-RES-PAK $ 120 / 5 x 1 mL
Methyl formate (2500 µg/mL)
5000 µg/mL in Water
1000 µg/mL each in MeOH 2 comps.
Tetrahydrofuran (1000 µg/mL)
Trifluoromethane (1000 µg/mL) o-Xylene o-Xylene-d10
Formamide
m-Xylene (1000 µg/mL)
o-Xylene (1000 µg/mL)
p-Xylene (1000 µg/mL) Instrument Performance Check PMI Labeled Standard Direct
Solution Injection
PMI Stock Standard C CLP-004-10X $ 10 / 1 x 1 mL M-1666A-DI-LAB 1 x 1 mL
CLP-004-10X-PAK SAVE 20% $ 40 / 5 x 1 mL 1000 µg/mL each in Water 6 comps.
M-1666A-SSC 1 x 1 mL
250 µg/mL in MeOH
1000 µg/mL each in MeOH 4 comps. Acetonitrile-d3 Methanol-d3
Butyl acetate Isopropyl acetate Dimethyl sulfoxide-d6 n-Propanol-1-d1
p-Bromofluorobenzene
Ethyl acetate Pentyl acetate Ethanol-d6 Tetrahydrofuran-d8
220 Quality System is Certified to comply with the International ISO 9001 Quality Standard
EPA Method 1667A Method 1667A
Pharmaceutical Waste Discharge Standards
NEW
Method 1667A Formaldehyde, Isobutyraldehyde & Furfural by Derivatization followed by HPLC for PMI pollutants
PMI Carbonyl & Carbonyl Derivative
Method 1665-1667A
PMI Derivatization Reagent
PMI Carbonyl DNPH Set
PMI Carbonyl Set
M-1667A-DERV-10ML-PAK $ 50 / 5 x 10 mL
M-1667A-DNPH-SET $ 65 / 3 x 1 mL
M-1667A-SET $ 40 / 3 x 1 mL
1.0 mg/mL in Ethanol
Set includes 3 individual products listed below
Set includes 3 individual products listed below
Each at 1.0 mg/mL in AcCN
Each at 1.0 mg/mL in AcCN
2,4-Dinitrophenylhydrazine (DNPH)
Formaldehyde-DNPH (M-1667A-01-DNPH)
Formaldehyde (M-8315-R3-10-10X)
2-Furaldehyde-DNPH (M-1667A-02-DNPH)
2-Furaldehyde (M-1667A-02)
Isobutyraldehyde-DNPH (M-1667A-03-DNPH)
Isobutyraldehyde (M-1667A-03)
Methods of Interest
PMI QA/QC Carbonyl Deriv.
PMI QA/QC Carbonyl Mix For Additional Pharmaceutical Discharge
Standards, see Methods 1671 and 1673
M-1667A-M $ 35 / 1 x 1 mL DNPH Mix
M-1667A-M-PAK $ 140 / 5 x 1 mL on page 224.
M-1667A-DNPH $ 60 / 1 x 1 mL
250 µg/mL each in AcCN 3 comps. M-1667A-DNPH-PAK $ 280 / 5 x 1 mL
Formaldehyde Isobutyraldehyde 250 µg/mL each in AcCN 3 comps.
2-Furaldehyde
Formaldehyde-DNPH
2-Furaldehyde-DNPH
Isobutyraldehyde-DNPH
221
AccuStandard � Tel. 800-442-5290 / 203-786-5290 � Fax 203-786-5287 � www.accustandard.com
EPA Method 1668
Method 1668
Method 1668 Congener Set - 209 Chlorinated Biphenyl Congeners by HRGC/HRMS
M-1668A-0.01X-SET $ 700 / 5 x 1 mL (M-1668A-1-0.01X, M-1668A-2-0.01X, M-1668A-3-0.01X, M-1668A-4-0.01X, M-1668A-5-0.01X)
Congener specific determination of all 209 chlorinated biphenyl congeners for calibration on a SPB-Octyl capillary column.
PCB Congener Mix 1 PCB Congener Mix 2
M-1668A-1-0.01X 1 x 1 mL M-1668A-2-0.01X 1 x 1 mL
At stated conc. in Isooctane 83 comps. At stated conc. in Isooctane 54 comps.
3-Chlorobiphenyl (2.5 µg/mL) 2,3',4,5,5'-Pentachlorobiphenyl (5.0 µg/mL) 2,4-Dichlorobiphenyl (2.5 µg/mL)
2,6-Dichlorobiphenyl (2.5 µg/mL) 2',3,4,5,5'-Pentachlorobiphenyl (5.0 µg/mL) 2,3-Dichlorobiphenyl (2.5 µg/mL)
2,5-Dichlorobiphenyl (2.5 µg/mL) 2,3,3',4,5-Pentachlorobiphenyl (5.0 µg/mL) 3,4-Dichlorobiphenyl (2.5 µg/mL)
2,3'-Dichlorobiphenyl (2.5 µg/mL) 2',3,3',4,5-Pentachlorobiphenyl (5.0 µg/mL) 2,2',5-Trichlorobiphenyl (2.5 µg/mL)
2,4'-Dichlorobiphenyl (2.5 µg/mL) 2,3,3',4,4'-Pentachlorobiphenyl (5.0 µg/mL) 2,3,6-Trichlorobiphenyl (2.5 µg/mL)
3,5-Dichlorobiphenyl (2.5 µg/mL) 3,3',4,5,5'-Pentachlorobiphenyl (5.0 µg/mL) 2,3,5-Trichlorobiphenyl (2.5 µg/mL)
3,3'-Dichlorobiphenyl (2.5 µg/mL) 2,2',3,5,6,6'-Hexachlorobiphenyl (5.0 µg/mL) 2,4,4'-Trichlorobiphenyl (2.5 µg/mL)
2,4,6-Trichlorobiphenyl (2.5 µg/mL) 2,2',3,3',6,6'-Hexachlorobiphenyl (5.0 µg/mL) 2,3,4'-Trichlorobiphenyl (2.5 µg/mL)
2,3',6-Trichlorobiphenyl (2.5 µg/mL) 2,2',3,4',5,6'-Hexachlorobiphenyl (5.0 µg/mL) 3,4',5-Trichlorobiphenyl (2.5 µg/mL)
2,4',6-Trichlorobiphenyl (2.5 µg/mL) 2,2',3,5,5',6-Hexachlorobiphenyl (5.0 µg/mL) 2,2',5,6'-Tetrachlorobiphenyl (5.0 µg/mL)
2',3,5-Trichlorobiphenyl (2.5 µg/mL) 2,2',3,4,5',6-Hexachlorobiphenyl (5.0 µg/mL) 2,2',4,6'-Tetrachlorobiphenyl (5.0 µg/mL)
2,3',5-Trichlorobiphenyl (2.5 µg/mL) 2,2',3,4,5,6'-Hexachlorobiphenyl (5.0 µg/mL) 2,3',5',6-Tetrachlorobiphenyl (5.0 µg/mL)
2,4',5-Trichlorobiphenyl (2.5 µg/mL) 2,2',3,4,5,6-Hexachlorobiphenyl (5.0 µg/mL) 2,2',4,5-Tetrachlorobiphenyl (5.0 µg/mL)
2',3,4-Trichlorobiphenyl (2.5 µg/mL) 2,2',3,3',5,5'-Hexachlorobiphenyl (5.0 µg/mL) 2,3,4,6-Tetrachlorobiphenyl (5.0 µg/mL)
3,3',5-Trichlorobiphenyl (2.5 µg/mL) 2,3,3',4,5',6-Hexachlorobiphenyl (5.0 µg/mL) 2,3',4',6-Tetrachlorobiphenyl (5.0 µg/mL)
3,4,5-Trichlorobiphenyl (2.5 µg/mL) 2,2',4,4',5,5'-Hexachlorobiphenyl (5.0 µg/mL) 2,3',4,5'-Tetrachlorobiphenyl (5.0 µg/mL)
3,3',4-Trichlorobiphenyl (2.5 µg/mL) 2,2',3,3',4,5'-Hexachlorobiphenyl (5.0 µg/mL) 2,3,3',5'-Tetrachlorobiphenyl (5.0 µg/mL)
2,2',4,6-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,5-Hexachlorobiphenyl (5.0 µg/mL) 2,3,4,5-Tetrachlorobiphenyl (5.0 µg/mL)
2,2',3,6-Tetrachlorobiphenyl (5.0 µg/mL) 2,3,4,4',5,6-Hexachlorobiphenyl (5.0 µg/mL) 2,3,3',4-Tetrachlorobiphenyl (5.0 µg/mL)
2,2',5,5'-Tetrachlorobiphenyl (5.0 µg/mL) 2,3,3',4,5,5'-Hexachlorobiphenyl (5.0 µg/mL) 2,3,4,4'-Tetrachlorobiphenyl (5.0 µg/mL)
2,2',4,5'-Tetrachlorobiphenyl (5.0 µg/mL) 2,3',4,4',5,5'-Hexachlorobiphenyl (5.0 µg/mL) 2,2',3,5,6'-Pentachlorobiphenyl (5.0 µg/mL)
2,4,4',6-Tetrachlorobiphenyl (5.0 µg/mL) 2,3,3',4,4',5-Hexachlorobiphenyl (5.0 µg/mL) 2,2',4,4',6-Pentachlorobiphenyl (5.0 µg/mL)
2,2',3,4-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,3',5,6,6'-Heptachlorobiphenyl (5.0 µg/mL) 2,2',3,4',6-Pentachlorobiphenyl (5.0 µg/mL)
2,3',5,5'-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,6,6'-Heptachlorobiphenyl (5.0 µg/mL) 2,3',4,5',6-Pentachlorobiphenyl (5.0 µg/mL)
2,3,3',5-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,3',5,5',6-Heptachlorobiphenyl (5.0 µg/mL) 2,2',3,4',5-Pentachlorobiphenyl (5.0 µg/mL)
2,3,4',5-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,5',6-Heptachlorobiphenyl (5.0 µg/mL) 2,2',4,4',5-Pentachlorobiphenyl (5.0 µg/mL)
2,3',4,4'-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,4,4',5',6-Heptachlorobiphenyl (5.0 µg/mL) 2,3,3',4,6-Pentachlorobiphenyl (5.0 µg/mL)
3,3',4,5'-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4',5,6-Heptachlorobiphenyl (5.0 µg/mL) 2,3,4',5,6-Pentachlorobiphenyl (5.0 µg/mL)
3,3',4,5-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,4',6-Heptachlorobiphenyl (5.0 µg/mL) 2,3,3',5,5'-Pentachlorobiphenyl (5.0 µg/mL)
3,4,4',5-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,5,5'-Heptachlorobiphenyl (5.0 µg/mL) 2,3,3',4,5'-Pentachlorobiphenyl (5.0 µg/mL)
2,2',3,6,6'-Pentachlorobiphenyl (5.0 µg/mL) 2,3,3',4,4',5',6-Heptachlorobiphenyl (5.0 µg/mL) 2,3',4,4',5-Pentachlorobiphenyl (5.0 µg/mL)
2,2',4,5',6-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,4',5-Heptachlorobiphenyl (5.0 µg/mL) 2,3,4,4',5-Pentachlorobiphenyl (5.0 µg/mL)
2,2',3,5',6-Pentachlorobiphenyl (5.0 µg/mL) 2,3,3',4,4',5,6-Heptachlorobiphenyl (5.0 µg/mL) 2,2',3,4',6,6'-Hexachlorobiphenyl (5.0 µg/mL)
2,2',3,4,6-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,5',6,6'-Octachlorobiphenyl (7.5 µg/mL) 2,2',3,4,6,6'-Hexachlorobiphenyl (5.0 µg/mL)
2,2',3,4,6'-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,4,4',5,6,6'-Octachlorobiphenyl (7.5 µg/mL) 2,2',3,3',5,6'-Hexachlorobiphenyl (5.0 µg/mL)
2,2',3,5,5'-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,5,6,6'-Octachlorobiphenyl (7.5 µg/mL) 2,2',3,4',5',6-Hexachlorobiphenyl (5.0 µg/mL)
2,3,3',5',6-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,5,5',6-Octachlorobiphenyl (7.5 µg/mL) 2,2',3,4,4',6-Hexachlorobiphenyl (5.0 µg/mL)
2,2',3,3',5-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,4',5',6-Octachlorobiphenyl (7.5 µg/mL) 2,2',3,3',4,6'-Hexachlorobiphenyl (5.0 µg/mL)
2,3',4,4',6-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,4',5,6-Octachlorobiphenyl (7.5 µg/mL) 2,3,3',5,5',6-Hexachlorobiphenyl (5.0 µg/mL)
2,2',3,4,5'-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,4',5,5'-Octachlorobiphenyl (7.5 µg/mL) 2,3',4,4',5',6-Hexachlorobiphenyl (5.0 µg/mL)
2,2',3,4,4'-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,4,4',5-Hexachlorobiphenyl (5.0 µg/mL)
2,2',3,3',4-Pentachlorobiphenyl (5.0 µg/mL) 2,3,3',4,5,6-Hexachlorobiphenyl (5.0 µg/mL)
2,2',3,3',4,4'-Hexachlorobiphenyl (5.0 µg/mL)
2,3,3',4',5,5'-Hexachlorobiphenyl (5.0 µg/mL)
PCB Congener Mix 3 2,3,3',4,4',5'-Hexachlorobiphenyl (5.0 µg/mL)
M-1668A-3-0.01X 1 x 1 mL 2,2',3,4,4',6,6'-Heptachlorobiphenyl (5.0 µg/mL)
At stated conc. in Isooctane 29 comps. 2,2',3,4,5,6,6'-Heptachlorobiphenyl (5.0 µg/mL)
2,2',3,4',5,5',6-Heptachlorobiphenyl (5.0 µg/mL)
3,4'-Dichlorobiphenyl (2.5 µg/mL) 2,2',3,4,5-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,4,5,5',6-Heptachlorobiphenyl (5.0 µg/mL)
2,2',4-Trichlorobiphenyl (2.5 µg/mL) 2,3,4,5,6-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,4,4',5,6-Heptachlorobiphenyl (5.0 µg/mL)
2,4,5-Trichlorobiphenyl (2.5 µg/mL) 2,3,3',4',5-Pentachlorobiphenyl (5.0 µg/mL) 2,3,3',4,5,5',6-Heptachlorobiphenyl (5.0 µg/mL)
2,3,3'-Trichlorobiphenyl (2.5 µg/mL) 2,2',4,4',5,6'-Hexachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,4',6,6'-Octachlorobiphenyl (7.5 µg/mL)
2,2',3,6'-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,4',5,6-Hexachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,5,5',6'-Octachlorobiphenyl (7.5 µg/mL)
2,3,5,6-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,4,4',6'-Hexachlorobiphenyl (5.0 µg/mL) 2,2',3,4,4',5,5',6-Octachlorobiphenyl (7.5 µg/mL)
2,3,3',6-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,4',5,5'-Hexachlorobiphenyl (5.0 µg/mL)
2,2',3,3'-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,4,5,5'-Hexachlorobiphenyl (5.0 µg/mL)
Method 1668 Congener Set
2,3',4,5-Tetrachlorobiphenyl (5.0 µg/mL) 2,3,3',4',5',6-Hexachlorobiphenyl (5.0 µg/mL)
2',3,4,5-Tetrachlorobiphenyl (5.0 µg/mL) 2,3,3',4,4',6-Hexachlorobiphenyl (5.0 µg/mL) Continued on Next page
3,3',5,5'-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,4,4',5,6'-Heptachlorobiphenyl (5.0 µg/mL)
2,2',3,5,6-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,5,6'-Heptachlorobiphenyl (5.0 µg/mL)
2,2',3,3',6-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,5,6-Heptachlorobiphenyl (5.0 µg/mL)
2,2',4,5,5'-Pentachlorobiphenyl (5.0 µg/mL) 2,3,3',4',5,5',6-Heptachlorobiphenyl (5.0 µg/mL)
2,3,3',5,6-Pentachlorobiphenyl (5.0 µg/mL)
222 Quality System is Certified to comply with the International ISO 9001 Quality Standard
EPA Method 1668 Method 1668
Method 1668 Congener Set - 209 Chlorinated Biphenyl Congeners by HRGC/HRMS (Continued)
PCB Congener Mix #4 PCB Congener Mix #5
M-1668A-4-0.01X 1 x 1 mL M-1668A-5-0.01X 1 x 1 mL
At stated conc. in Isooctane 15 comps. At stated conc. in Isooctane 28 comps.
2,3',4-Trichlorobiphenyl (2.5 µg/mL) 2,2',3',4,6-Pentachlorobiphenyl (5.0 µg/mL)
2-Chlorobiphenyl (2.5 µg/mL)
Method 1668
2,3,4-Trichlorobiphenyl (2.5 µg/mL) 2',3,4,5,6'-Pentachlorobiphenyl (5.0 µg/mL)
4-Chlorobiphenyl (2.5 µg/mL)
2,3',4,6-Tetrachlorobiphenyl (5.0 µg/mL) 2,3,3',4',6-Pentachlorobiphenyl (5.0 µg/mL)
2,2'-Dichlorobiphenyl (2.5 µg/mL)
2,2',4,4'-Tetrachlorobiphenyl (5.0 µg/mL) 3,3',4,4',5-Pentachlorobiphenyl (5.0 µg/mL)
4,4'-Dichlorobiphenyl (2.5 µg/mL)
2,2',3,4'-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',4,4',6,6'-Hexachlorobiphenyl (5.0 µg/mL)
2,2',6-Trichlorobiphenyl (2.5 µg/mL)
2,3,4',6-Tetrachlorobiphenyl (5.0 µg/mL) 2,2',3,4,4',5'-Hexachlorobiphenyl (5.0 µg/mL)
2,2',3-Trichlorobiphenyl (2.5 µg/mL)
2,3',4',5-Tetrachlorobiphenyl (5.0 µg/mL) 3,3',4,4',5,5'-Hexachlorobiphenyl (5.0 µg/mL)
3,4,4'-Trichlorobiphenyl (2.5 µg/mL)
2,2',4,5,6'-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,4',5,6,6'-Heptachlorobiphenyl (5.0 µg/mL)
2,2',6,6'-Tetrachlorobiphenyl (5.0 µg/mL)
2,2',3',4,5-Pentachlorobiphenyl (5.0 µg/mL) 2,3,3',4,4',5,5'-Heptachlorobiphenyl (5.0 µg/mL)
2,2',3,5-Tetrachlorobiphenyl (5.0 µg/mL)
2,3,4,4',6-Pentachlorobiphenyl (5.0 µg/mL) 2,2',3,3',5,5',6,6'-Octachlorobiphenyl (7.5 µg/mL)
2,2',3,5'-Tetrachlorobiphenyl (5.0 µg/mL)
2',3,4,4',5-Pentachlorobiphenyl (5.0 µg/mL) 2,3,3',4,4',5,5',6-Octachlorobiphenyl (7.5 µg/mL)
2,4,4',5-Tetrachlorobiphenyl (5.0 µg/mL)
2,2',3,3',5,6-Hexachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl (7.5 µg/mL)
2,3,3',4'-Tetrachlorobiphenyl (5.0 µg/mL)
2,2',3,3',4,6-Hexachlorobiphenyl (5.0 µg/mL) 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl (7.5 µg/mL)
3,3',4,4'-Tetrachlorobiphenyl (5.0 µg/mL)
2,3,3',4',5,6-Hexachlorobiphenyl (5.0 µg/mL) Decachlorobiphenyl (7.5 µg/mL)
2,2',4,6,6'-Pentachlorobiphenyl (5.0 µg/mL)
2,2',3,4,4',5,5'-Heptachlorobiphenyl (5.0 µg/mL)
Level of Chlorination Calibration / Spike Set
M-1668A-LOC-SET $ 150 / 2 x 1 mL (M-1668A-NAT, M-1668A-PAR)
Determination of Chlorobiphenyl content at each level of chlorination
Native PCB Calibration Mix PAR PCB Spike Mix
M-1668A-NAT 1 x 1 mL M-1668A-PAR 1 x 1 mL
At stated conc. in Isooctane 19 comps. At stated conc. in Isooctane 19 comps.
4-Chlorobiphenyl (5 µg/mL) 4-Chlorobiphenyl (10 µg/mL)
4,4'-Dichlorobiphenyl (5 µg/mL) 4,4'-Dichlorobiphenyl (10 µg/mL)
2,4,4'-Trichlorobiphenyl (5 µg/mL) 2,4,4'-Trichlorobiphenyl (10 µg/mL)
3,3',4,4'-Tetrachlorobiphenyl (0.2 µg/mL)
3,3',4,4'-Tetrachlorobiphenyl (1 µg/mL)
2,3,3',4,4'-Pentachlorobiphenyl (10 µg/mL)
2,3,3',4,4'-Pentachlorobiphenyl (5 µg/mL)
2,3,4,4',5-Pentachlorobiphenyl (10 µg/mL)
2,3,4,4',5-Pentachlorobiphenyl (5 µg/mL)
2,3',4,4',5-Pentachlorobiphenyl (10 µg/mL)
2,3',4,4',5-Pentachlorobiphenyl (5 µg/mL)
2',3,4,4',5-Pentachlorobiphenyl (10 µg/mL)
2',3,4,4',5-Pentachlorobiphenyl (5 µg/mL)
3,3',4,4',5-Pentachlorobiphenyl (1 µg/mL)
3,3',4,4',5-Pentachlorobiphenyl (5 µg/mL)
2,3,3',4,4',5-Hexachlorobiphenyl (10 µg/mL)
2,3,3',4,4',5-Hexachlorobiphenyl (10 µg/mL)
2,3,3',4,4',5'-Hexachlorobiphenyl (10 µg/mL)
2,3,3',4,4',5'-Hexachlorobiphenyl (10 µg/mL)
2,3',4,4',5,5'-Hexachlorobiphenyl (10 µg/mL)
2,3',4,4',5,5'-Hexachlorobiphenyl (10 µg/mL)
3,3',4,4',5,5'-Hexachlorobiphenyl (2 µg/mL)
3,3',4,4',5,5'-Hexachlorobiphenyl (10 µg/mL)
2,2',3,3',4,4',5-Heptachlorobiphenyl (2 µg/mL)
2,2',3,3',4,4',5-Heptachlorobiphenyl (10 µg/mL)
2,2',3,4,4',5,5'-Heptachlorobiphenyl (10 µg/mL)
2,2',3,4,4',5,5'-Heptachlorobiphenyl (10 µg/mL)
2,3,3',4,4',5,5'-Heptachlorobiphenyl (2 µg/mL)
2,3,3',4,4',5,5'-Heptachlorobiphenyl (10 µg/mL)
2,2',3,3',4,4',5,5'-Octachlorobiphenyl (10 µg/mL)
2,2',3,3',4,4',5,5'-Octachlorobiphenyl (10 µg/mL)
2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl (10 µg/mL)
2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl (10 µg/mL)
2,2',3,3',4,4',5,5',6,6'-Decachlorobiphenyl (20 µg/mL)
2,2',3,3',4,4',5,5',6,6'-Decachlorobiphenyl (20 µg/mL)
Method 1668A - Combined Congener Standard
NEW
M-1668A-C-NT-LOC-WD $ 150 / 1 x 1 mL
20 µg/mL each in Isooctane 33 comps.
2-Chlorobiphenyl 2,2',4,4',6,6'-Hexachlorobiphenyl
4-Chlorobiphenyl 2,3,3',4,4',5-Hexachlorobiphenyl
2,2'-Dichlorobiphenyl 2,3,3',4,4',5'-Hexachlorobiphenyl
4,4'-Dichlorobiphenyl 2,3',4,4',5,5'-Hexachlorobiphenyl
2,2',6-Trichlorobiphenyl 3,3',4,4',5,5'-Hexachlorobiphenyl
2,3,5-Trichlorobiphenyl 2,2',3,3',4,4',5-Heptachlorobiphenyl
2',3,5-Trichlorobiphenyl 2,2',3,4,4',5,5'-Heptachlorobiphenyl
3,4,4'-Trichlorobiphenyl 2,2',3,4,4',5,6'-Heptachlorobiphenyl
2,2',6,6'-Tetrachlorobiphenyl 2,2',3,4',5,5',6-Heptachlorobiphenyl
3,3',4,4'-Tetrachlorobiphenyl 2,2',3,4',5,6,6'-Heptachlorobiphenyl
3,4,4',5-Tetrachlorobiphenyl 2,3,3',4,4',5,5'-Heptachlorobiphenyl
2,2',4,6,6'-Pentachlorobiphenyl 2,2',3,3',5,5',6,6'-Octachlorobiphenyl
2,3,3',4,4'-Pentachlorobiphenyl 2,3,3',4,4',5,5',6-Octachlorobiphenyl No. 1290
2,3,4,4',5-Pentachlorobiphenyl 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl
Vacuum dessicator
2,3',4,4',5-Pentachlorobiphenyl 2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl
2',3,4,4',5-Pentachlorobiphenyl 2,2',3,3',4,4',5,5',6,6'-Decachlorobiphenyl
3,3',4,4',5-Pentachlorobiphenyl
223
AccuStandard � Tel. 800-442-5290 / 203-786-5290 � Fax 203-786-5287 � www.accustandard.com
EPA Method 1671 & 1673
Method 1671
1673
Method 1671 Volatile Organic Compounds Specific to Method 1673 Polyethylene glycol - 600 by Deriv. & HPLC
the Pharmaceutical Mfr. Industry by GC/FID
Poly(ethylene glycol)-600
M-1673 $ 35 / 1 x 1 mL
PMI Internal Standard M-1673-PAK SAVE 20% $ 140 / 5 x 1 mL
M-1671A-IS $ 20 / 1 x 1 mL 2.5 mg/mL in Tetrahydrofuran
M-1671A-IS-PAK SAVE 20% $ 80 / 5 x 1 mL
Polyethylene glycol-600
1.0 mg/mL in Water
Tetrahydrofuran
Surrogate Standard
M-1673-SS $ 25 / 1 x 1 mL
M-1673-SS-PAK SAVE 20% $ 100 / 5 x 1 mL
PMI Standard Direct Injection
1.0 mg/mL in Tetrahydrofuran
M-1666A-DI $ 20 / 1 x 1 mL
At stated conc. in Water 12 comps. Diethylene glycol monohexyl ether
Acetonitrile (1000 µg/mL) Formamide (5000 µg/mL)
Diethylamine (2500 µg/mL) Methanol (1000 µg/mL)
Derivatization Reagent
Dimethylamine (1000 µg/mL) 2-Methoxyethanol (1000 µg/mL)
M-1673-DERV-5ML $ 30 / 1 x 5 mL
Dimethyl sulfoxide (1000 µg/mL) Methylamine (2500 µg/mL)
10 mg/mL in Tetrahydrofuran
Ethanol (1000 µg/mL) 1-Propanol (1000 µg/mL)
Ethylene glycol (2500 µg/mL) Triethylamine (2500 µg/mL) 3,5-Dinitrobenzyl chloride
Custom Formulations
Contact our Technical Service department for different
composition PEG materials. AccuStandard can obtain
PEG with different mixtures of oligomers having molecular
weights centered around 200, 300, 400, 550, 1000, 1450,
3350, 8000, 10,000 ca.
Technical Note
AccuStandard maintains a full QA/QC
Laboratory with the following types of
instruments to insure the quality of our
standards. GC/FID, GC/ECD, GC/
NPD, GC/MS, P & T GC/MS, HPLC,
and IC.
224 Quality System is Certified to comply with the International ISO 9001 Quality Standard
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